A solution of the desired quantity of the material is produced in water or well prepared as directed during the pharmacopoeia in Nessler’s cylinder; incorporate two ml dilute hydrochloric acid except wherever hydrochloric acid is Employed in the planning of the solution. Dilute it to forty five ml with drinking water, add five ml of barium sulpha

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If modifications for the method take place, the evaluation of their effect on the method’s suitability for its intended use is crucial. g. specific consideration should be paid to particulars which include sonication time, sonication bath temperature and mixing and to samples exactly where demixing is known to arise).Exam of System suitability